Alexa Roberts _ Final Masters Thesis_ETD Submission
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Alexa Roberts _ Final Masters Thesis_ETD Submission
IMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submissionin Chemical EngineeringCleveland State University43586Submitted in fulfillment of requirements for the degreeMASTER OF SCIENCE IN BIOMEDICAL ENGINEERINGAt the CLEVELAND STATE UNIVERSITY44317We hereby approve this thesis forALEXA ROBERTSCandidate for the Master of Science in Biomedical Engineering de Alexa Roberts _ Final Masters Thesis_ETD Submissiongree for theDepartment of Chemical and Biomedical EngineeringAnd the CLEVELAND STATE UNIVERSITY’SCollege of Graduate Studies byThesis Chairperson. ChaAlexa Roberts _ Final Masters Thesis_ETD Submission
ndrasekhar Kothapalli. Ph.D.Department of Chemical & Biomedical EngineeringDepartment & DateThesis Committee Member. Geyou Ao. Ph.D.Department of ChemIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submissionse: May 3. 2021ACKNOWLEDGEMENTS1 would like to thank Dr. Chandra Kolhapalli for the opportunity to participate in this research project and the continuous guidance he has given me in all aspects of the lab work". T would like to acknowledge the entire Chemical and Biomedical Engineering Department f Alexa Roberts _ Final Masters Thesis_ETD Submissionor then assistance throughout the program, for partially supporting my tuition and stipend through teaching assistantships, and the opportunities to pAlexa Roberts _ Final Masters Thesis_ETD Submission
resent and discuss my research project with other interested students and faculty. 1 would like to acknowledge Dr. Petal Fodor and Dr. Geyou Ao for thIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submission and imaging. Besides, the devices used in this project were developed in collaboration with Dr. Petal Fodor. I would like to thank Dr. Kiril Streletzky and Samantha Tietjen for their assistance on the DLS analysis, as well as Ana Dilillo and Fjorela Xhyliu for assistance on the NS3 NanoSpectralyzer Alexa Roberts _ Final Masters Thesis_ETD Submission equipment. 1 would like to acknowledge the access to equipment in Dr. Ao’s lab. Finally. I would like to recognize my numerous lab colleagues in Dr.Alexa Roberts _ Final Masters Thesis_ETD Submission
Kolhapalli’s lab al Cleveland Stale University. Ĩ would like to thank Gautam Mahajan for guiding me through some protocols and providing me with assisIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submissiond Marissa Sarslicld for her explanation and recommendations toward the procedure and time management of the project. Finally. Ĩ would like toacknowledge the present and past group members: Rushik Bandodkar. Tahir Butt.Ben Bosela, and Quinton Wright.IMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIM Alexa Roberts _ Final Masters Thesis_ETD SubmissionIZATION OF POLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSABSTRACTNanoparticles have a wide range of applications in biomedicine,Alexa Roberts _ Final Masters Thesis_ETD Submission
catalysis, energy, semiconductors, and consumer products, to name a few. Conventionally, batch synthesis of a variety of nanoparticles is achieved usIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submission bottom-up approaches, could be time and resource intensive when optimizing for the effects of reaction parameters and their interplay on nanoparticle characteristics and purity. Microfluidic platforms could help overcome these limitations byenabling high-throughput reactions, combinatorial approach Alexa Roberts _ Final Masters Thesis_ETD Submissiones, in situ monitoring capabilities, and utilizing fewer reactant volumes. The aim of this study is to optimize the synthesis of three different typesAlexa Roberts _ Final Masters Thesis_ETD Submission
of nanomaterials: poly-lactic-co-glycolic acid (PLGA) nanoparticles, gold (AuNPs) nanoparticles, and lead iodide perovskite nanoplatelets (PNPs). usiIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science i Alexa Roberts _ Final Masters Thesis_ETD Submission flowrate into the device ports, reactant compositions and mole ratios, and mixer type was investigated to identify the optimal synthesis conditions, i.e.. the conditions leading to narrow and uniform size distributions, for each type of nanomaterial in these micromixers. The outcomes from these mic Alexa Roberts _ Final Masters Thesis_ETD Submissionrofluidic mixers were compared to their counterparts from batch synthesis. Future studies could test the applications of such nanoparticles in targeteAlexa Roberts _ Final Masters Thesis_ETD Submission
d imaging and drug encapsulation.IMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science iIMPLEMENTATION OF MICROFLUIDIC MIXERS FOR THE OPTIMIZATION OFPOLYMERIC. GOLD. AND PEROVSKITE NANOMATERIALS SYNTHESISALEXA ROBERTSBachelor of Science iGọi ngay
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