Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
➤ Gửi thông báo lỗi ⚠️ Báo cáo tài liệu vi phạmNội dung chi tiết: Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) cal and Preparative PurposesBYJOHAN LINDHOLMACTA UNIVERSITATIS ƯPSALIENSIS UPPSALA 2004https://khothuvien.cori!Dissertation presented at Uppsala University to be publicly examined in Room 1542, BMC, Uppsala, Friday. September 24. 2004 at 13:15 for the degree of Doctor of Philosophy. The examination Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) will be conducted in Swedish.AbstractLindholm. J. 2004. Development and Validation of HPLC Methods for Analytical and Preparative Purposes. .Acta UnivJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
ersitatis Upsalicnsis. Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995. 87 pp. Uppsala ISBN 91-554-600Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) reas: (i) analysis of biotechnological synthesis and (ii) determination of adsorption isotherm parameters. There is today a lack of detailed recommendations for analytical procedures in the field of biotechnological production of drugs. Therefore, guidelines were given for analytical development and Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) validation in this field; the production of 9a-hydroxyprogcstcronc was used as model. In addition, a rapid method using IIPLC coupled with diodc-arraJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
y-dclcction (DAD) and mass spectrometry (MS), was developed for the preliminary identification and quantification of the product. In addition, requireComprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) the precision and accuracy of the quantitative method were considerably improved.Preparative chromatography is a powerful separation method for the purification of pure compounds from more or less complex sample mixtures. One such mixture can be the process liquid from a fermentation, another examp Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) le can be a racemic mixture of compounds whose enantiomeric constituents must be isolated. Computer-assisted modeling can be used to optimize preparatJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
ive chromatography. However, competitive adsorption isotherm parameters are required as input data for the computer simulations. In this thesis, a newComprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) etitive adsorption isotherm parameters from a broad concentration range. With the new mctlMxl die determination of adsorption isotherm parameters from a quaternary mixture could be done for the first lime, rhe profiles simulated with these parameters showed excellent agreement with the corresponding Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) experimental profiles, validating the accuracy of the adsorption isotherm parameters derived by the new method.Keywords: High performance liquid chroJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
matography (IIPLC). Analytical biotechnology. Sample preparation, Diodc-array-dctcction (DAD). Mass spectrometry (MS). Validation. Preparative chromatComprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) psala. Sweden£ Johan Lindholm 2004ISSN II04-232XISBN 91-554-6005-4um:nbn:sc:uu:diva-4442 (http:.'',um.kb.sci‘rcsolvc?um^urn:nbn:sc:uu:diva-4442)•I'ilTrninafiraidrar ỪCÍI min a is fade LinnéaList of PapersThis diesis IS based on the following papers, which are referred to in the text by then Roman nu Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) merals I-VI:I.Use of liquid chromatography-diode-array detection and mass spectrometry for rapid product identification in biotechnological synthesisJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
of a chiral steroid.Johan Lindholm. Douglas Westerlund, Karl-Enk Karlsson. Karin Caldwell and Toigny Fomstedt. Journal of Chromatography A. 992 (2003)Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) l.Johan Lindholm. Monika Johansson and Torgny Fornstedt Journal of Chromatography B. 791 (2003). 323-336.III.Investigation of the adsorption behaviour of a chiral model compound on Kromasil CHI-TBB.Johan Lindholm and Torgny Fomstedt. Manuscript.IV.Theoretical and experimental study of binary pertuba Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) tlon peaks with focus on peculiar retention behaviour and vanishing peaks in chiral liquid chromatography.Patrik Forssen. Johan Lindholm and Torgny FoJohan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1)
mstedt. Journal of Chromatography A. 991 (2003). 31-45.V.Validation of the accuracy of the perturbation peak method for determination of single and biComprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for Analytic Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) of the accuracy of the perturbation peak method for determination of multi-component adsorption isotherm parameters in LC.Johan Lindholm. Patrik Forssen and Torgny Fomstedt. Accepted June 2004 in Analytical Chemistty.Reprints were made with kind permission from publishers. Johan lindholm development and validation of hplc methods for analytical and preparative purposes acta universitatis upsaliensis 2004 (1) Comprehensive Summaries of Uppsala Dissertations from the Faculty of Science and Technology 995Development and Validation of HPLC Methods for AnalyticGọi ngay
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