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Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

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Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) gyThis book is printed on acid-free paper. 00Copyright o 2001 by John Wiley & Sons. Inc. All rights reserved.Published simultaneously in Canada.No par

t of this publication may be reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic, mechanical, photocopying Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

, recording, scanning, or otherwise, except as permitted under Sections 107 or 108 of the 1976 United States Copyright Act, without either the prior w

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

ritten permission of the Publisher, or authorization through payment of the appropriate per-copy fee to the Copyright Clearance Center. 222 Rosewood D

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) t. John Wiley & Sons. Inc., 605 Third Avenue. New York. NY 10158-0012. (212) 850-6011. fax (212) 850-6008. E-Mail: PERMREQ@WILEY.COM.For ordering and

customer sendee, call 1-800-CALL-WILEY.Library of Congress Cataloging in Publication Data:Nishimura, ShigeoHandbook of heterogeneous catalytic hydroge Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

nation for organic synthesis / Shigeo Nishimura.p. cm.Includes bibliographical references and indexes.ISBN 0-471-39698-2 (cloth : alk. paper)I. Hydrog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

enation. 2. Catalysis. 3. Organic compounds—Synthesis. 1. Title.ỌD281.H8N57 2001Amno n,1T7.-lAPREFACECatalytic hydrogenation is undoubtedly the most u

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) ratories and industrial processes. Almost all catalytic hydrogenations have been accomplished using heterogeneous catalysts since the earliest stages.

Homogeneous catalysts have been further developed and have extended the scope of catalytic hydrogenation, in particular, for highly selective transfo Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

rmations. However, heterogeneous catalysts today continue to have many advantages over homogeneous catalysts, such as in the stability of catalyst, ea

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

se of separation of product from catalyst, a wide range of applicable reaction conditions, and high catalytic ability for the hydrogenation of hard-to

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) xamples are included here where highly selective hydrogenations have been achieved over heterogeneous catalysts, typically in collaboration with effec

tive additives, acids and bases, and solvents.Examples of the hydrogenation of various functional groups and reaction pathways are illustrated in nume Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

rous equations and schemes in order to help the reader easily understand the reactions. In general, the reactions labeled as equations are described w

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

ith experimental details to enable the user to choose a pertinent catalyst in a proper ratio to the substrate, a suitable solvent, and suitable reacti

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) action pathways as well as the selectivity of catalysts, although the difference between equations and schemes is not strict. Simple reactions are som

etimes described in equations without experimental details. Comparable data are included in more than 100 tables, and will help the user understand th Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

e effects of various factors on the rate and/or selectivity, including the structure of compounds, the nature of catalysts and supports, and the natur

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

e of solvents and additives. A considerable number of experimental results not yet published by the author and coworkers can be found in this Handbook

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) (to a limited extent) are also included. The hydrogenations of industrial importance have been described with adequate experimental and mechanistic d

etails.The references quoted here are by no means comprehensive. In general, those thatxĩi PREFACEIam grateful to the authors of many excellent books Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

to which I have referred during preparation of this book. These books are listed at the end of chapters under “General Bibliography.”I wish to express

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

my thanks to the libraries and staff of The Institute of Physical and Chemical Research. Wako. Saitama and of Tokyo University of Pharmacy and Life S

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001) s book. I thank Professor Emeritus Michio Shiota of Ochanomizu University and Professor Yuzuru Takagi of Nihon University for their helpful discussion

s. Special thanks are due to my three children who provided me with a new model personal computer with a TFT-LC display for preparing the manuscript a Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

nd to my wife Yasuko. who had continuously encouraged and supported me in preparing and publishing this book until her death on November 28. 1999.SH1G

Shigeo nishimura handbook of heterogeneous catalytic hydrogenation for organic synthesis wiley interscience (2001)

EO NishimuraHachioji. TokyoCONTENTSPrefacexi1Hydrogenation Catalysts11.1Nickel Catalysts21.1.1Reduced Nickel31.1.2Nickel from Nickel Formate5

HANDBOOK OF HETEROGENEOUS CATALYTIC HYDROGENATION FOR ORGANIC SYNTHESISSHIGEO NISHIMURAProfessor EmeritusTokyo University of Agriculture and Technolog