Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

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Nội dung chi tiết: Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

Tokyo Institute of TechnologyGraduate School of Bioscience and BiotechnologyDepartment of BioengineeringMatsuda LaboratoryLiquid carbon dioxide as a s

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols superior solvent lorCandida antarctica lipase B catalyzed kinetic resolution of sec-alcoholsThesis submitted for the degree ofMaster of EngineeringbyH

oang Nam Hai42186IndexIndexIndex.................................................................................iAbbreviations....................... Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

................................................iiiChapter 1Introduction...............................................................1Chapter 2Candi

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

a anlarciica lipase B catalyzed kinetic resolution of roc-l-phcnylclhanol in liquid carbon dioxide....................................................

Tokyo Institute of TechnologyGraduate School of Bioscience and BiotechnologyDepartment of BioengineeringMatsuda LaboratoryLiquid carbon dioxide as a s

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols s for large-scale biosynthesis ofoptically pure compounds....................................................82.2.1KR of 1 -phenylethanol in a continu

ous-flow stirred-tank reactor (CSTR) usingliquid CO:..................................................................92.2.2K.R of 1-phenylethanol in Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

a continuous packed - bed reactor (CPBR) using liquidCO:.........................................................................122.3Comparison of th

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

e productivity of continuous-flow and batch reactors using liquidCO: as an medium............................................................14Chapter

Tokyo Institute of TechnologyGraduate School of Bioscience and BiotechnologyDepartment of BioengineeringMatsuda LaboratoryLiquid carbon dioxide as a s

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols ...............183.1Substrate specificity of CAI.-B catalyzed transesterification of alcohols..183.2Expanding substrate scope of CAL-B using liquid CO

:........................19Chapter 4Conclusion and perspective................................................25Chapter 5Experimental section......... Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

.............................................264.1Chemicals and instrument...................................................264.2General procedure fo

Liquid carbon dioxide as a superior solvent for candida antarctica lipase b catalyzed kinetic resolution of sec alcohols

r preparation of rnc-alcohols..........................274.3General procedure for preparation of acetates..............................294.4General pr

Tokyo Institute of TechnologyGraduate School of Bioscience and BiotechnologyDepartment of BioengineeringMatsuda LaboratoryLiquid carbon dioxide as a s