Structure elucidation by modern NMR a workbook
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Structure elucidation by modern NMR a workbook
Structure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook y J. B. Stothers andK. NakanishiProf. Dr. Helmut Duddeck Dr. Wolfgang Dietrich Fakultat fur Chemie Ruhr-Univcrsităt Bochum Postfach 102148 4630 Bochum, FRGDie Deutsche Biblwthek - ClP-EmheitsaufnahmcDuddeck, Helmut:Structure elucidation by modern NMR : a workbook / H Duddeck ; w. Dietrich. With pref Structure elucidation by modern NMR a workbook , by J. B. Stothers and K. Nakanishi. -2.. rev. and cnl. cd. - Darmstadt: Steinkopff; New York : Springer. 1992Dt. Ausg. u.d.T: Duddcck. Helmut: StrukStructure elucidation by modern NMR a workbook
turaufkUrung mit modemer N M R-SpektroskopieISBN-13. 978-3-7985-0930-6e-lSBN-13 978-3-442-97787-9Dot. 10.1O077578-3-642.97787-9NE: Dietrich, Wolfgang:Structure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook tion, reprinting, re-use of illustrations, recitation, broadcasting, reproduction on microfilms or in other ways, and storage in data banks. Duplication of this publication or parts thereof is only permitted under the provisions of the German Copyright Law of September 9, 1965, in its version of Jun Structure elucidation by modern NMR a workbook e 24. 1985, and a copyright fee must always be paid. Violations fall under the prosecution act of the German Copyright Law.Copyright © 1992 by Dr. DieStructure elucidation by modern NMR a workbook
trich Stcinkopff Vcrlag GmbH & Co. KG. DarmstadtChemistry Editor: Dr. Mana Magdalene Nabbc - Copy Editing: Marilyn Salmansohn. James c. Willis -ProducStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook hat such names arc exempt from the relevant protective laws and regulations and therefore free for general use.ForewordFor several years, we have been organizing seminars and workshops on the application of modem one-and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Structure elucidation by modern NMR a workbook Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry.In 1987, we wStructure elucidation by modern NMR a workbook
rote a workbook (Strukturauíklárung mil modemer NMR-Spcktroskopie. Steinkopff. Darmstadt. FRG, 1988) in German language based on our experience in theStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook tent. The response of readers and discussions with colleagues from many countries encouraged US two years later to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in Engli Structure elucidation by modern NMR a workbook sh version. Now, after the rapid development of basic multipulse NMR methods in the early 1980s, the avantgardc in modem NMR is concentrating on the iStructure elucidation by modern NMR a workbook
nvention and optimization of advanced techniques, e.g., three-dimensional experiments. For the beginners, however, the situation has not changed markeStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook ease the number of exercises from 23 to 33. the new ones being basically single-spectrum-problcms.This book could not have been written in the present form without the help of a number of colleagues and, therefore, we acknowledge gratefully the generous supply of samples from and useful discussions Structure elucidation by modern NMR a workbook with B. Abcgaz (Addis Ababa. Ethiopia), u. H. Brinker (Bingham, New York. USA), E. Dagne (Addis Ababa, Ethiopia), M. Gonzalez-Sierra (Rosario, ArgentiStructure elucidation by modern NMR a workbook
na), J. Harangi (Debrecen, Hungary), s. A. Khalid (Khartoum. Sudan). A. Lévai (Debrecen. Hungary), M. A. McKcrvcy (Cork, Ireland). M. Michalska (Lodz.Structure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook FRG), J. Wicha (Warsaw. Poland) und K. Wieghardt (Bochum, Germany).We also thank Martin Gartmann, Monika Hiegemann, Harald Kiihne, Dr. Doris Rosenbaum. Elsa Sauerbier, and Peter Walff for their committed cooperation, their assistance in the measurements, and in the preparation of the figures.Inspite Structure elucidation by modern NMR a workbook of painstaking efforts mistakes can hardly be avoided. Vré are always grateful for any response from readers to correct or improve the text.If we havStructure elucidation by modern NMR a workbook
e been successful in conveying an impression of the wealth of information offered by modern NMR, then the book has satisfied its goal.Bochum, FRG, MarStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook R is by far the most widely used. It is used in practically every phase of research in chemistry and biochemistry, including tertiary structural investigations of biopolymers, e.g., nucleic acids, peptides, proteins, carbohydrates, etc., in solution. More recently the technique of solid state NMR ha Structure elucidation by modern NMR a workbook s even started to reveal very subtle structural information of noncrystalline samples. With the rapid advancements seen in new measurement techniquesStructure elucidation by modern NMR a workbook
and instrumentation (a 600 MHz 'H-NMR is becoming a fairly common equipment seen in many industrial and academic institutions), NMR will continue its Structure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook y are well aware of the various basic NMR techniques at their disposal. The era in which decoupling, NOE measurements, and straightforward 2D measurements of proton and carbon NMR sufficed is long over. The scientist must not only have a reading knowledge of the potentialities of NMR spectroscopy, b Structure elucidation by modern NMR a workbook ut has to have real experience in problem solving. The more they are exposed to such experience, the more efficient and elegantly can they apply NMR sStructure elucidation by modern NMR a workbook
pectroscopy to day-to-day research problems. It is a fact that unless being involved daily in structure-solving projects, not many chemists have suffiStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook olfgang Dietrich, with long experience in teaching NMR through problem solving, have now expanded their highly successful First Edition. The book familiarizes the readers with the various NMR techniques by step-wise solving of 33 structural problem sets rather than through texts. In this respect, it Structure elucidation by modern NMR a workbook is totally unique. The monograph consists of a brief inưoduction, a 24 page outline of NMR methodology, a 137 page presentation of 33 exercises, a 10Structure elucidation by modern NMR a workbook
page outline of strategic approaches for proHem solving, and finally an 88 page solution section. It is written in very common language and from a toStructure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces by Structure elucidation by modern NMR a workbook biochemists who may be familiar with biopolymers but have not had the opportunity to solve structural problems of complex organic natural products.New York, August 1992K. Nakanishi Structure elucidation by modern NMR a workbook Structure Eluãdation by Modem NMRH. Duddeck, w. DietrichStructure Elucidation by Modern NMRA Workbook2nd, revised and enlarged editionWith Prefaces byGọi ngay
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