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Designed synthesis of novel metal organic frameworks for photocatalysts application

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Nội dung chi tiết: Designed synthesis of novel metal organic frameworks for photocatalysts application

Designed synthesis of novel metal organic frameworks for photocatalysts application

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application PLICATIONDOCTORAL DISSERTATIONHOCHIMINH CITY 2017VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNB ERSITY HOC HIMINH CITYHA LAC NGUYENDESIGNED S

YNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOCATALYST APPLICATIONMajor subject: TECHNOLOGY FOR ORGANIC COMPLEXESMajor subject code: 62527505Ind Designed synthesis of novel metal organic frameworks for photocatalysts application

ependent Referee 1: Prof Dr. Khoa Cuu NGUYENIndependent Referee 2: Assoc. Prof. Dr. Huven Thanh PHAMReferee 1: Assoc. Prof. Dr. Tuan Anh vuReferee 2:

Designed synthesis of novel metal organic frameworks for photocatalysts application

Assoc. Prof. Dr. Hoang Thai NGUYENReferee 3: Assoc. Prof. Dr. Quan Thanh PHAMSUPERVISORS1. Prof. Dr. Nam Thanh Son PHAN2. Dr. Danh Thanh TONGPROTESTAT

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application rch, and the author had done the truthtill science and contributed to the development progress of science. Any claim and conclusion were cited by the

references and documented papers, rhe author recognized that the seriousness and authenticity need to be strongly considered.AuthorIla Lac Nguyen1ABST Designed synthesis of novel metal organic frameworks for photocatalysts application

RACTOver the past two decades, the prominent growth of Metal Organic Frameworks (MOFs). a high ordered and porous materials class had been receiving t

Designed synthesis of novel metal organic frameworks for photocatalysts application

he pay attention by the research community specially. Constructing by Secondary Building Units (SBUs) of metal clusters and organic linkers combinatio

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application ts chemistry) which can be tunable the structural features (e.g.. pore size, porosity) to make MOFs address the environment problems as well as the ta

rgeted applications such as gas uptake, separation, catalyst, drug deliver}', water treatment. In term of MOFs synthesis, the plenteous chemistry of m Designed synthesis of novel metal organic frameworks for photocatalysts application

etal and controllability of organic linkers were exploited to make the uncountable amount of new MOFs material. In this case, the simple solvothermal

Designed synthesis of novel metal organic frameworks for photocatalysts application

reaction or other methods (e.g., hydrothermal, solvent free, slow dispersion) was usually employed to obtain new MOFs. This method for MOFs synthesis

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application h predicting structures is now commonplace, a robust and modular synthetic approach to designing new MOF materials remains elusive as a result of the

trial-and-error nature of crystallization processes, a lack of control over crystallization, and the regular discoveries of multiple crystalline phase Designed synthesis of novel metal organic frameworks for photocatalysts application

products once the reaction is complete. In MOF chemistry. the building block method, whereby discrete, preassembled metal 0X0 clusters are reacted wi

Designed synthesis of novel metal organic frameworks for photocatalysts application

th well-defined organic linkers, has been utilized to achieve a greater degree of control over MOF construction. However, the isolation and subsequent

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application ciation of ligands, limits the applicability of this method Additionally. It IS far from given that the desired MOF structure will be obtained as meta

l 0X0 building blocks have been observed to rearrange during the synthesis Means of overcoming this lack of total synthetic control is to take inspira Designed synthesis of novel metal organic frameworks for photocatalysts application

tion from molecular synthesis, in which certain conditions have been discovered to achieve specific end products. In this contribution, we articulate

Designed synthesis of novel metal organic frameworks for photocatalysts application

a strategy for making discrete metal clusters in situ that areiiappropriately functionalized to affect imine condensation reactions, commonly used in

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application ome the challenge of synthetic incompatibility. rhe structural features of targeted material, termed MOF-901. was fully characterized powder X-ray dif

fraction and supplemental analyses. As a result of the incorporation of Ti(IV) units. MOF-901 was proven to be photocatalytically active and was appli Designed synthesis of novel metal organic frameworks for photocatalysts application

ed to the photocatalyzed polymerization of methyl methacrylate (MMA).For further investigation, the photocatalysis properties of MOF which is isorclic

Designed synthesis of novel metal organic frameworks for photocatalysts application

ular to MOF-901 structure, MOF-902 was successfully synthesized by enlarging the linking unit, and applied to the application of polymerization reacti

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application MOF-902. the molecular weight of polyMMA IS as high as the value of polyMMA which IS produced by MOF-901 catalyst, and the poly dispersity index of po

lyMMA produced by MOF-902 catalyst IS lower than MOF-901 (1.27 compared to 1.60).Moreover, we have successfully synthesized three novel MOFs termed MO Designed synthesis of novel metal organic frameworks for photocatalysts application

F-903(Fe). MOF-904(Fe), and VNU-18(Cu) based on triangular Iron (III) cluster and extraordinary three discrete Cu(II) building units, respectively. Th

Designed synthesis of novel metal organic frameworks for photocatalysts application

ese materials were frill characterized by the powder X-ray diffraction, single crystal X-ray diffraction analysis, thcrmogravimclric analysis, gas ads

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

Designed synthesis of novel metal organic frameworks for photocatalysts application y, which arc proven by Nitrogen isotherm al 77 K al low pressure.ill

VIETNAM NATIONAL ƯNIVERSITY-HOCHIMINH CITYBACH KHOA UNIVERSITYHA LAC NGUYENDESIGNED SYNTHESIS OF NOVEL METAL-ORGANIC FRAMEWORKS FOR PHOTOC ATALYST APP

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