Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
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Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
A TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) ry Department, Woolwich Polytechnic ;Sometime Beit Scientific Research Fellow of the Imperial College, LondonWith diagrams and 8 photographsTHIRD EDITIONLONGMANLONGMAN GROUP LIMITED LondonAssociated companies, branches and representatives throughout the worldFirst published 1948 New impression with Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) minor corrections. October 1948Second Edition 1951New impression with addition of Chapter Xll on Semimicro Technique 1954Third Edition. /956New impresArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
sion with corrections and additions 1957New impressions 1959. 1961. 1962. 1964. 1965. 1967. 1970. 1972. and 1974ISBN 0 582 44245 1PRINTED IN GREAT BRIA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) students and practising organic chemists has encouraged the author to undertake an exhaustive revision of the entire text in the light of the numerous developments in practical organic chemistry since the book was first written (1945-46). The net result has been an increase in the length of the volu Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) me by some 150 pages, a figure which gives some indication of the new matter incorporated in the present edition.It is impossible within the limitatioArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
ns of a short preface to give a detailed list of the numerous changes and additions. Some of the more important new preparations include :1.Chapter IIA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) 11,90); ion exchange resin catalyst method for esters (111,102); acetamide (urea method) (111,107); ethyl a bromopropionate (111,126); acetoacetatic ester oondensation using sodium triphenylmethide (111,151).2.Chapter IV. a Chloromethylnaphthalene (IV,23); benzylamine (Gabriel synthesis) (IV,39); TY Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) TV-dialkylanilines (from amines and trialkyl orthophos pilates) (IV,42); a naphthaldehyde (Sommelet reaction) (IV,120); a phenyl cinnamic acid (PerkinArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
reaction using triethylamine) (IV,124); 3-nitrostyrene (IV,129); p-bromonaphthalene and 3 naphthoic acid (from 2 naphthylamine 1 sulphonic acid) (IV,A TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) 2 ; 5 dimethyl- and 2 : 4-dimethyl-dicarbethoxy-pyrrole (V,12-V,13); 2-amino- and 2 : 4 dimethyl-thiazole (V,15~V,16); 3:5-dimethyl-pyrazole (V,17); 4-ethylpyridine (from pyridine) (V,19) ; n amyl pyridines from picolines) (V,28) ; picolinic, nicotinic and iaonicotimc acid (V,21-V,22); (ethyl nicot Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) inate and 3 cyanopyridine (V,23 v,24); uramil (V,25); 4-methyl-(coumarin (V,28); 2-hydroxy lepidine (V,29).4.Chapter VI. Reductions with potassium borArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
ohydridc (VI,11); Oppen-auer oxidation (VI,13) ; epoxidation and hydroxylation of ethylenic compounds (VI,15); Arndt Eistert reaction (VI,17); DarzensA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) 23); Stobbe condensation (VI,24); Willgerodt reaction (VI»25); unsymmetrical diaryls (VI,27); syntheses with organolithium compounds (VI,28); syntheses with organosodium compounds (VI,29); syntheses with organocadmium compounds (VI,30); some electrolytic syntheses (VI,31); chromatographic adsorption Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) (VI,33); ring enlargement with diazomethane (VI34).5.Chapters VII-IX. Diazomethane (p tolylsulphonylmethylnitrosamide method) (VII30) ; Girard’s reagArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
ents “ T ” and “ p ” (VII,25) ; pseudo saccharin chloride (VII,26); 2 : 2'-dipyridyl (VIII,13); ninhydrin (VIII,14); 3-indoleacetic acid (IX,14).A newA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) ay be modified in the near future, it is hoped that the brief treatment scattered throughout the volume will stimulate the student’s interest in this important branch of organic chemistry. It will be noted that many reactions are designated by name ; this may be undesirable on pedagogical grounds bu Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) t, in most cases, established usage and the example set by the various volumes of Organic Reactions (J. Wiley) may be put forward in justification.viPArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
REFACE TO THIRD EDITIONChapter XII is concerned with Semimicro Technique. There can be little doubt that preparations on a smaller scale than has hithA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) ing laboratories and also in training for research. Once the student has mastered the special technique, no difficulty should be experienced in adapting most of the preparations described in the book to the semi-micro scale. A few examples of small-scale preparations are included together with a sug Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) gested list of experiments for an elementary course.Section A,7, “ Applications of infrared and ultraviolet absorption spectra to organic chemistry,”Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
should provide a brief introduction to the subject.It is regretted that the size of the volume has rendered the insertion of literature references impA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) ture introduced in response to requests by many readers. The volume comprises virtually at least three books under one cover, viz., experimental technique, preparations, and qualitative organic analysis. It should therefore continue to be of value as a one volume reference work in the laboratory. St Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) udents at all levels will find their requirements for laboratory work (excluding quantitative organic analysis) adequately provided for and, furthermoArthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974)
re, the writer hopes that the book will be used as a source of information to supplement their theoretical studies.The author wishes to thank Dr. G. HA TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of Chemistr Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) estions ; Dr. G. H. Jeffery for invaluable assistance in numerous ways ; and c. Kyte, B.Sc., and R. Grezskowiak, B.Sc., for a number of original preparations and also for checking and improving many of the new experimental procedures. Arthur israel vogel a text book of practical organic chemistry including qualitative organic analysis third edition longman (1974) A TEXT BOOK OFPRACTICAL ORGANIC CHEMISTRYINCLUDINGQUALITATIVE ORGANIC ANALYSISByARTHUR I. VOGEL, D.Sc.(Lond.),D.I.C.,F.R.I.C.Formerly Head of ChemistrGọi ngay
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